Polymer Solutions Incorporated
   
Polymer Solutions Incorporated (PSI) is an independent laboratory and a strategic global resource for chemical analysis, physical testing, research and development services, and litigation services.

We are ISO-17025 accredited, cGMP compliant, FDA registered and DEA licensed.

 
    PSI Building 
Polymer Solutions Incorporated
2903C Commerce Street
Blacksburg, VA 24060
540-961-4300 | 1-877-961-4341
www.PolymerSolutions.com
 
 

October 2009

Aging and Chemical Resistance Testing of Plastic and Rubber Products



It is important to verify chemical compatibility of plastic and rubber materials to be sure the materials will perform properly in specific application. Materials are exposed to a variety of chemicals, temperatures, radiation, and mechanical stress.

There are methods available to assure the performance of a material before it is released. Of significant importance is the ability to not only assess chemical compatibility but also to accelerate the response of plastics and rubber materials to the chemical challenge.

And, if a material failure does occur in the field, analytical methods can reveal the root cause. For example, chemical resistance testing of pipe sections has been performed.
> Read more


Contamination Analysis

The surface of a plastic product, the interior of a rubber molded product, or a raw ingredient, process solvent, or additive may contain unintended chemical compounds. Contamination may cause functional problems, cause a product to look ugly, or be of no consequence depending on the amount and type.

Sensitive analysis methods, together with proper sampling techniques, can isolate and identify contamination. Armed with data, one can take rational steps to determine the source of the contamination and eliminate it.

For example, FTIR spectroscopy has been used to identify inclusions in molded products.
> Read more

Molecular Weight Analysis

The processing and end-use performance of plastic parts depends heavily on the molecular weight of the plastic itself.

Polymers inherently have a distribution of chain lengths resulting in a molecular weight distribution. Lower molecular weight chains help improve melt processing, while the higher molecular weight fraction can be critical to mechanical properties.

A variety of molecular weight analysis techniques specific to material type, industry served and information required are used at Polymer Solutions incorporated. We will help you choose the one that is right for you.
> Read more


Deformulation Analysis

Need to know batch-to-batch variations in raw materials? How about understanding the ingredients in a competitor's product? Worried about a possible patent infringement? What about a comparison of good vs. bad products? Let us answer these and other questions for you!

In one case, we deformulated a specialty protective coating.
> Read more



In this issue:


We bring you chemical analysis, physical testing and molecular systems information you can use to better understand how analysis may help you fully characterize the materials you work with!

  • Aging and Chemical Resistance Testing
  • Contamination Analysis
  • Extractables and Leachables Analysis
  • Molecular Weight Analysis
  • Polymer Structure Analysis
  • Deformulation Analysis
  • Jay’s Cool Microscopy Pics of the Month

Jay's Cool SEM Pics


Extractables and Leachables Analysis




Packaging and medical products are two industries that have a high interest in understanding the extractable and leachable content of their materials. Some specific applications have government-required tests that must be performed to assure consumer safety. In other cases, a manufacturer wants to understand the behavior of materials in the operating environment.

Protocols are available to extract or leach chemical compounds from polymers, plastics, and rubber materials. And, sensitive and chemically-specifiic analysis methods are used to determine the identity and amount of extractables and leachables.

Elastomer tubing used in pharmaceutical manufacturing operation, for example, is tested for leachables.
> Read more


Polymer Structure Analysis


Polymer blends and copolymer systems are utilized in many industrial applications including medical implants, packaging, injection molded parts, adhesives, and coatings. Fourier Transform Infrared Spectroscopy (FTIR) can be used to analyze polymer samples, raw materials, and blends. Nuclear Magnetic Resonance Spectroscopy (NMR) provides highly detailed chemical structure information that can be used to enhance the FTIR spectral data sets.



Copolymer compositions and identifications of unknown polymers are accomplished using these techniques.
> Read more


Jay’s Cool Microscopy Pics of the Month


In his day to day life leading the PSI Microscopy lab, Jay works with some extremely interesting materials. They are even more fascinating at high magnification. Here, Jay shares some of his favorites. In this month’s edition of the PSI newsletter, he shares some pictures that include (left to right). Click on each image to view it in higher resolution.

1. Scanning Electron Microscopy (SEM) image of an ABS (acrylonitrile-butadiene-styrene) polymer sample

2. Atomic Force Microscopy (AFM) image of the ABS polymer sample.

3. Transmission Electron Microscopy (TEM) image of the ABS polymer sample.
 


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Cool Chemistry Links


Zero Gravity

At Polymer Solutions, we pride ourselves on being experts in the fields of Chemistry, Chemical Engineering and Materials Science. Many of us have spent years developing our collective knowledge base. Along the way, we have all grown to have a deep interest in science. Here, we share what we think are interesting science experiments that many of us have performed during our training, or on the side, due to personal interest.

This month’s video demonstrates viscoelastic effects in a sphere of water in zero gravity, an air bubble in the water sphere, water droplets in the air bubble in the water sphere . . .
 
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